DiProbe Technology

When coupled to an FTIR the newly introduced DiProbe technology provides an unique capability for monitoring smaller scale reactions taking place in less accessible reactors which may be located in tighter spaces than state of the art remote FTIR probes. It is highly resistant to attack by corrosive or abrasive chemicals and enables direct measurement of reactants, intermediates, by-products and products formed or consumed during a chemical reaction. Additionally the very small sample probe diameter allows sampling directly in containers with narrow openings.

Features of the DiProbe:

  • Diamond ATR element
  • 2 x 45° internal reflections
  • Transmission from 3 µm to 18 µm
  • Diameter: 6mm
  • Hastelloy shaft
  • Chemical inert sealing
  • Shaft length: up to 50cm
  • Fiber cable length: up to 5m; SMA connectors
  • Temperature Range: up to 100°C

Product Features

Benefits

ATR based technology

Allows spectra to be collected from a small volume of liquid and eliminates sample quench and pretreatment

In-situ capability

Eliminates off-line sampling and greatly increases the amount of data that may be collected per unit time

DiProbe sensors can be interfaced to a fiber length of up to 5m

Affords outstanding flexibility when positioning instruments in laboratories, pilot plants and plants.

High throughput single fiber technology is used

Up to 4 Probes can be coupled to 1 FTIR

Chemical compatibility of a diamond ATR element

Allows reaction/process monitoring in challenging chemical environments at high and low temperature and at high pressure

Probe body and seal constructed from Hastelloy and inert brazings

No corrosion whatever the chemical environment

6mm probe head size

Enables to interface the probe to reactors where space or volume is limited

Probe availability in overall lengths of 5 to 50cm

Permits integration of probes into all kind of vessels, pipes, flow cells and drain valves.

Reproducibility

Consistent spectral performance over time

High flexibility

Alignment and optical throughput are assured whatever the conformation of the fiber cable

Low weight

Ease of use

No purge required

Since reduced path length of the IR radiation traveling through, the absorption bands due to water vapor and CO2 are diminished.

Affordable price

Affordable Price: Existing FTIR Equipment can be used








DiProbe Sensitivity (metering of ethanol with acetic-acid-ethyl-ester)





Spectral Grade Fiber Cables

  • Structure: core/clad
  • Composition: AgCl/AgBr
  • Diameter: 0.9mm/1mm , others on request
  • Refractive index: 2.2
  • Numerical Aperture: 0.5
  • Max. Lengh: 5m
  • Attenuation @10µm: 0.2 dB/m
  • Attenuation @5µm : 0.4 dB/m
  • Attenuation @3µm : 0.8 dB/m
  • Connectors: SMA type
  • Housing: PEEK
  • Cabling: Single fiber or bundle
  • Temp. Range: 10°C to 80°C, in special housings:-100°C up to +200°C
  • Bending radius: > 15cm